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  • Infections, Cleaning and Sanitation

    Folks--

    I am fighting a brewhouse infection. Given the fact that our lab procedures/equipment have lagged behind our enthusiastc production/demand I am in the unenviable position of having to kill everything without really knowing where in the process it was introduced. To that end, today I have CIP'd the kettle, WP, heat exchanger and mash tun with a sodium hydroxide based cleaner at 3% dilution at 170 deg for 45 minutes. Tomorrow I will CIP all of the aforementioned components with a nitric acid/phosphoric acid blended cleaner for 45 minutes, also for 45 minutes. Following that I will sanitize all with peracitic acid. I have inspected all gaskets. Until I have evidence that the beasts are under control this is the cleaning regimen I intend to maintain. Also, and perhaps most importantly we have some rudimentary lab procedures in place so that we can track our progress (wort sample before and after heat exchanger, FV samples, BT samples and so forth). Finally, I got rid of all the yeast and am starting over.

    Any comments or recommendations?

    Some questions:

    In what condition do you leave your brewhouse after cleaning, ie:

    Drain valves open or closed?

    Manway doors open or closed?

    Manway gaskets installed or stored?

    Drain valves attached or removed?

    Racking valves attached or removed?

    Do you dissemble and soak the perlick valves during each cleaning?

    Heat exchanger -- full of liquid or empty? If full, what liquid?


    Thanks!

    Damien

  • #2
    Damien,

    Not knowing your Brewery size or procedures, i would recommend the following as well:

    1.) Dump your yeast and start fresh.

    2.) Disassemble the Heat Exchanger and clean each leaf in caustic. Oftentimes, especilly of you use whole leaf hops, you can get some chunks wedged up in there. Once a brew film has started growing on the leaves, it doesn't just CIP off. I have had to scrub ours, and we disassemble pretty regularly.

    3.) If you filter your beer, check the media and the filter itself. I know several brewer's who have witnessed shorter than usual shelf times due to the filter adding contaminants while filtering out the yeast.

    4.) If you use straight side Sankeys, check your keg washing procedures. There are whole discussions on this, but the washer must pulse to clean and sanitize the outside of the spear properly.

    Just a few humble thoughts..........

    Comment


    • #3
      I've also found running 200+ degree F water through EVERYTHING from the kettle to the fermenters quite effective. You can kill bugs with heat that won't be adequately touched by chemicals...

      Good luck!!!

      Tim

      Comment


      • #4
        First-remember your brewhouse need not be sanitized before the heat exchanger. Don't try to provide breeding grounds, but anything before the HX is mostly immaterial.
        Double vote on disassembling heat exchanger. If there are hop pieces poached in delicious wort that are wedged in nooks and crannies, chemicals can never sanitize it. (And if you were a wort/beer eating nasty, wouldn't you enjoy a vacation there?)
        How clean and porous is your aeration stone, and has wort (now spoiled) backed up into the oxygen hose?
        I found butterfly valve seats that were not sound in my brewery, and now check each one as it is up for cleaning. Very shocking to have one nearly crumble upon dissasembly. A little finger inserted inside to feel if the seat is smooth seems to work-otherwise they are a perfect hangout for nasties to "chill" waiting for their next meal. Also visually check for growth around where handle shaft goes thru valve body on both sides as a sign of leakage and a nasty resevoir. Valve seats are the perfect nasty habitat if every obvious other thing is perfectly clean, yet they seem so impervious to nasties without close inspection.
        Perhaps the thermostat or thermometer used to gauge sterilization got whacked and isn't reading correctly anymore. Happens way too often.

        Comment


        • #5
          My two cents:
          if you take 10 minutes more in your brewday to be obsessive about sanitizing, and that makes you sleep comfortably at night, DO IT.
          I spray the living daylights out of my TC fittings before transferring beer, filtering, anything. I sleep well at night, knowing I did everything possible (for me) to make wort and yeast happy! I soak things in Iodophor, not for the nice deep orange stain, but to know that bugs are dead. It makes me sleep well.
          I cycle acid then iodophor through my filter, knowing I've minimized bug counts - hence making me feel good about the brew I'm about to filter. I sleep well.
          "By man's sweat and God's love, beer came into the world" -- St. Arnold of Metz

          Comment


          • #6
            I also believe the brewhouse CIP cycles your using most likely will not clear up your sanitation issues. I would think your infection is post heat exchanger in the brewhouse or elsewhere in the cellar (hoses, tanks, etc..) Once you establish your Critical Control Points (CCP) you should be able to pinpoint an area of micro. infection. I'll do my best to answer the questions you have:

            In what condition do you leave your brewhouse after cleaning, ie:

            Drain valves open or closed?

            We leave all drain valves open on the brewhouse vessels. The WK, WH and Heat Exchanger are CIP'ed everynight. The rest of the brewhouse is CIP'ed after the brewing week is over.

            Manway doors open or closed?

            Manyway doors are closed after tank has been CIP'ed and sanitized. Doors on BH vessels are always closed.

            Manway gaskets installed or stored?

            Since the tanks are closed the manway gaskets are installed. Note that the manway gaskets for tanks are hand cleaned every use, sanitized and put back onto tank after CIP.

            Drain valves attached or removed?

            Drain valves are attached during CIP but occassionally removed prior to CIP to inspect or replace valve lining.

            Racking valves attached or removed?

            Racking valves are removed and scrubbed and then placed back into tank for CIP.

            Do you dissemble and soak the perlick valves during each cleaning?

            Yes, every time. Soaked in sanitizer before reassembling tank after CIP.

            Heat exchanger -- full of liquid or empty? If full, what liquid?

            Heat exchanger is left full after daily CIP. During the week hot water is sanitizer after caustic CIP. At the end of week packed with sanitizer.

            This system works well. It is also "checked" frequently as every brew length a sterile wort sample is collected for micro plating. CCP's are plated frequently and fermenter are plated.

            As previously mentioned the entire brewhouse is CIP'ed at the end of the week. This also includes dissembling wort aeration equipment and cleaning and sanitizing equipment. The aeration filter is SS so it is autoclaved to guarantee sterilization.

            As Rob mentioned--soaking tubs are nice for parts. One tub for cleaning, one tub for sanitizing.

            When CIP'ing your heat exchanger make sure your flow rate is close to the flow rate you chill your wort. If you think it's plugged or fouled run a CIP in reverse to help loosen any chunks. This might make all the difference or at least make hand cleaning of each plate a little easier.

            Good luck and I hope you're successful in ridding the source of infection.

            MJ
            Mike Jordan
            Brewmaster
            Boxing Cat Brewery
            Shanghai, P.R. China
            michael@boxingcatbrewery.com

            Comment


            • #7
              Many excellent suggestions, another potential culprit can be beer stone in fermenters and serving tanks, especially in the manway shadows. Beer stone can harbor some real nasty creatures deep in the stone that sanitizer may not penetrate to. A good visual inspection with a heavy hot acid wash will clear it up quite quickly.
              Good Luck

              Comment


              • #8
                Cleaning

                I also agree with Moonlight and Mike J(we met at GT and CDA brewing-always nice to have one of the "big boys" on this little forum!). I have seen only one problem area in a brewhouse in my 16 yrs. of experience, many problems elsewhere. Make sure you are getting at least 1 1/2-2x the process flow with cleaners thru your heat x., or else it will require frequent breakdowns. Always take apart everything possible when doing CIP, soaking any part that is not a part of the "pumping" process- always visually inspect any CIP'd equipment. Leave things open to drain overnight, or pack with a sanitizer. We may be "brewmasters", but it has always seemed to me that a "CIP master" is an often overlooked/underrated part of any brewing job. Good Luck!

                Paul Thomas
                Bitter Root Brewing
                Paul Thomas
                Brewer
                Sockeye Brewing
                www.sockeyebrew.com

                Comment


                • #9
                  Thank you all!

                  Folks--

                  Thank you all so much for your great advise. Of note, our heat exchanger was full of junk, mostly hop leaf debris.

                  After a thorough cleaning (entire brewhouse) we brewed again and the forced wort sample is still clear after 96 hours. Also sampled with HLP media and clear at 96 hours.

                  Every other recommendation was implemented as well and we feel alot better.

                  Thanks again,
                  Damien

                  Comment


                  • #10
                    Also, I'd recommend that the cleaning cycle for your pumps, hoses and heat exchanger be in reverse, that is to backflush your heat exchanger. I've always done it that way, and I find it does a particularly good job of flushing out all the nasties that lodge in there. We'd very occasionally take the HE apart to inspect it, and it was pretty much always clean as a whistle...

                    Cheers, Tim

                    Comment


                    • #11
                      I'm with Tim on this one -- it's my practice to alternate forward and reverse (i.e. backflushed) caustic cycles on my HX. Periodically, I'll throw in a hot acid loop in it to minimize beerstone.

                      Cheers!
                      "By man's sweat and God's love, beer came into the world" -- St. Arnold of Metz

                      Comment


                      • #12
                        I'm also with tim and rob on this one.The HX is usually the problem.I always do a 3 step clean in reverse flow with p.b.w then acid rinse, and pack with chlorine dioxide. Make sure hose is higher than top of HX to make sure all areas are being contacted !!!! Good Luck!!!!!!!!!

                        Comment


                        • #13
                          also, this may be elementary to cleaning the Hx, but there's the "filling the crossovers" - technique, using your pbw/or whatever - run it thru hot, then throttle your output back as low as possible to allow the pump to pack that sucker, shut it down, backflush in the morning. That helped a ton.

                          I like taking samples whenever I can. I have a very small system (bop kettles) and no lab, so I by name brand water bottles at the gas station - dump, and fill from output hose, and cap. I think that's far more sterile than anything I could get in the brew house.

                          hope this went well, the thread was very informative.

                          Comment


                          • #14
                            Hot water will kill everything in its path...

                            except that undersea bacteria that lives near lava flows
                            www.Lervig.no

                            Comment


                            • #15
                              Doesn't the hot water bakes on protein globs that will then be very very difficult to remove, other than disassembling and srubbing.

                              Comment

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